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Beilstein J. Org. Chem. 2016, 12, 2556–2562, doi:10.3762/bjoc.12.250
Graphical Abstract
Scheme 1: Synthesis of c3A described by Rousseau et al. in 1966 [22]. a) 1,2,3,5-Tetraacetyl-ß-D-ribofuranose, ch...
Scheme 2: Synthesis of c3A described by Montgomery et al. in 1977 [23]. The final step, displacement of the 2-chl...
Scheme 3: Synthesis of tribenzoylated 6-azido-3-deazapurine nucleoside 2. a) LiN3 (1.3 equiv), N,N-dimethylfo...
Scheme 4: Efficient 5-step synthesis of 3-deazaadenosine phosphoramidite 8 from commercially available, affor...